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device wafer during the thinning processes.
The final Si has a TTV around 70nm—
identical to the thickness variation of the
epitaxially-grown Si layer. The wafers are
then ready for nano-TSV processing.
Nano-TSV formation
The TSV process flow is shown in
Figure 4. The TSV patterning is done
by through-Si alignment and needs to
ensure that the nano-TSVs are aligned
to the bottom metal 1 (M1) layer. This
requires <20nm of overlay tolerance.
The TSVs have a 180 x 250nm oblong
top CD and are 500nm deep (the final
thickness after the thinning steps). TSV
etching is also carried out on the SPTS
Figure 3: Si thickness and TTV of the device wafer across the thinning process steps. Rapier™ XE system, this time using a
Bosch process with short cycle times
grown on a 300mm Si wafer and a 500nm ~20nm. The wet etch selectivity of Si to the to minimize the sidewall scalloping
capping layer of epitaxial Si is grown on top. SiGe is not high enough that wet etching and assist with subsequent depositions.
This Si capping layer is the starting point could be used for the entire Si removal. The The TSV etch needs to stop on a thin
for device fabrication. The SiGe content, aim of the dry etching is to get close enough dielectric layer that covers M1 as this
being SiGe25%, is selected as a compromise to the SiGe layer to allow the wet etch to avoids metal re-sputtering during TSV
between wet etch selectivity to Si (being stop within the SiGe and not breach it. The over-etching, which could otherwise
higher for higher Ge concentration) and SiGe layer thickness also has to be at least lead to device reliability issues [4].
film defectivity (being lower for lower Ge 50nm to prevent that. Finally, the SiGe layer After TSV etching, 10nm of oxide
concentration because of lattice mismatch). itself is wet etched, using a highly SiGe- is deposited conformally by plasma-
Following the above substrate preparation, to-Si selective chemical etchant, exposing enhanced atomic layer deposition
the next step is the fabrication of front-end- the epitaxial 500nm-thick Si layer. Figure (PEALD) throughout the TSV. Then
of-line (FEOL) devices in the 500nm thick Si 3 shows the Si thickness and TTV of the the TSV and M1 liners are etched in a
capping layer. The top (device) wafer and a
carrier wafer are then face-to-face dielectric
bonded using a combination of 150nm SiO
and 50nm of SiCN on both faces.
After wafer-to-wafer (W2W) bonding,
the next part of the process flow is shown
in Figure 2. The top wafer is thinned by
grinding to 50µm. Grinding is mechanically
damaging to the Si surface and sub-surface,
therefore the remaining Si thickness should
be larger than the affected Si thickness,
as cracks and disclocations must be
prevented from reaching the active device
areas, because they would impact device
performance and reliability. A further 1µm is
then polished from the Si by CMP to smooth
the surface. Then a dry etch step removes a
further 39µm of Si to leave 10µm above the
SiGe layer. Dry etching benefits from being
a high-rate step that avoids any mechanical
contact to the wafer. It also allows for in
situ thickness monitoring by near-infra-red
(NIR) interferometry. After dry etching,
the remaining Si has a TTV around 2µm.
Dry etching is fast (~9µm/min) but is not
selective to SiGe. Therefore, a wet etch is
needed to remove the remaining 10µm of Si
to the SiGe. The wet etching compensates Figure 4: TSV patterning process flow: a) Through Si-TSV alignment to bottom M1 and dry etch, stop on STI; b)
for the 2µm TTV leaving a SiGe TTV at PEALD oxide liner deposition (10nm) and liner etch (TSV) bottom; c) TSV metallization (Cu electroplating) and Cu
CMP; d) Back-side metal processing (BSM1).
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